From: Don WanamakerDate: June 24, 2009 11:00:10 AM EDT Subject: Re: [DCHAS-L] Wastewater testing Julie, Also determine if your POTW is the "control authority" for EPA's Pretreatment Program (40 CFR Part 403). You may need to submit a "baseline monitoring report" (to either the POTW, the Indiana Environmental Agency, or the EPA Region - depending on who's the Control Authority). If so, follow the applicable requirements for "new sources". Good luck. djw Don Wanamaker Environmental Management, Ltd. 845-429-1141 == From: dlwcihcsp**At_Symbol_Here**hotmail.com Subject: RE: [DCHAS-L] 3 RE: [DCHAS-L] Wastewater testing Date: June 24, 2009 11:28:13 AM EDT I might also add that if the regulatory agencies are going to be involved, they will require you to have the analyses performed by an independent laboratory. In house labs are generally considered to have a bias. There are also proficiency program requirements. So, before you spend a fortune setting this up, check to be sure you will not have to send them to an approved laboratory for the regulator to accept them. You can usually find a list of approved labs on your state environmental protection department's website. Donna Donna L. Wilson, CIH-CSP IH Resources 5923 Phillips Avenue Pittsburgh, PA 15217-2121 Telephone 412-521-3643 Cellular 412-576-7620 dlwcihcsp**At_Symbol_Here**hotmail.com == From: "Dr Henry" Date: June 24, 2009 11:53:22 AM EDT Subject: Re: [DCHAS-L] Wastewater testing Without knowing your levels, it would be difficult to pin down. For the list you give, ICP with a microwave digester is the best general method. One run does all the metals. If you have ultralow limits then ICP-MS may be needed. Although some may recommend it, I say stay away from GFAA. Spend the little extra on ICP-MS and get less headache. There are now low end models out there and some deals to be had in this economy Mercury is on your list takes a separate machine. You best bet for all this is to talk to the lab you are using now and get their advice. They know your limits and what is current in your state and permits. It is the permit methods in your location that should be used. Dr.Henry A. Boyter Jr. Director of Research Institute of Textile Technology NC State University College of Textiles Box 8301 2401 Research Drive Raleigh, NC 27695-8301 919-513-7704 http://www.itt.edu "Ride, boldly ride," The shade replied,-- "If you seek for Eldorado!" == FROM: jimmykwok**At_Symbol_Here**RAM-CHEM.COM Subject: Re: [DCHAS-L] Wastewater testing Dear All, The AAS is the best to use if your wastewater is with many oil or grease at ppm level. It is easy to clean the atomizer. Anyway the metal concentration is below 2ppm in the wastewater, so you have to run the sample without dilution , then it takes the risks of blocking . if there has more than 200ppm in the wastewater , so the sample should have 1 to 100 dilution factor , so the risk of blocking is less than 2 ppm . You have to use different gases in the AAS for Cd and Pb . The ICP is OK to use without many different AA lamps and different gases for Cd and Pb; but you have to take the pretreatment on oil and grease TDS , total suspended solid , as these will block the atomizer. The pretreatment is to take precipitation out of the TDS and Oil/ grease and filtered prior to the ICP dilution sample preparations . It is very common in the Analytical Lab in this application. Jimmy Kwok
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