Consider taking a metal tray and putting a steam coil underneath. Limit the steam pressure to a temperature below the flash point. Put it in the hood or a ventilated enclosure and it is inherently safe.
Richard Palluzi
PE, CSP
Pilot plant and laboratory consulting, safety, design,reviews, and training
www.linkedin.com/in/richardppalluzillc/
Richard P Palluzi LLC
72 Summit Drive
Basking Ridge, NJ 07920
rpalluzi**At_Symbol_Here**verizon.net
908-285-3782
From: ACS Division of Chemical Health and Safety <DCHAS-L**At_Symbol_Here**PRINCETON.EDU> On Behalf Of Ellen M. Sweet
Sent: Monday, February 25, 2019 10:20 AM
To: DCHAS-L**At_Symbol_Here**PRINCETON.EDU
Subject: [DCHAS-L] polymer curing question
Hi everyone,
I have a question from one of our researchers here at Cornell. Here’s the background:
“The process involves synthesizing and curing a novel polymer, PDMS based PU, onto plastic “coupons” which will have DFM evaporating off.
The cure process is intended to have the polymer form onto the surface of the coupons in a thin coat and make the surface non-binding.”
Our question is how to do this safely? DMF has a flash point of 58=B0C and a vapor density of 2.52.
A known method for this curing process is to place the plastic coupons into a flammable oven that is under vacuum and flushed with nitrogen.
Can anyone suggest another method that doesn’t involve the use of an oven like this? The group would have to purchase one to the tune of $50,000!
Thanks, Ellen
Ellen Sweet
Laboratory Ventilation Specialist
Department of Environmental Health and Safety, Cornell University
American Chemical Society, Division of Chemical Health and Safety
315-730-8896
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