Jyllian
The device will perform well for 1 mL titrations and perhaps up to 10 mL reactions, beyond that it will be difficult to use and offer no advantage over a canula.
The device will require some practice to learn to use and careful attention to proper procedure - that is to say, it will need operator training.
Finally, it has an equipment barrier to use that a lab will need to commit to overcoming.
Bottom line - I see an incremental advantage for small scale pyrophor use. For the application described - a teaching lab, it does make sense.
Thanks for bringing this to our attention.
Neal
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From: ACS Division of Chemical Health and Safety <DCHAS-L**At_Symbol_Here**PRINCETON.EDU> On Behalf Of Jyllian Kemsley
Sent: Tuesday, June 12, 2018 7:06 AM
To: DCHAS-L**At_Symbol_Here**PRINCETON.EDU
Subject: [DCHAS-L] New procedure for transferring tert-butyllithium from Sure/Seal bottles
Hi all,
Curious to know what people think of the tBuLi transfer procedure proposed in this paper just accepted by OPRD:
Compared to, say, the one in the ChemUCSD videos:
Thanks!
Jyllian
Jyllian Kemsley, Ph.D.
Executive Editor, Policy
Chemical & Engineering News
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