There is a huge body of literature on making nitrating acid solutions and for safely carrying out nitrations. Bretherick is certainly the starting place, but a good search on Science Direct and SciFinder is called for. Then, before you do bench work, develop an SOP and go over it in detail with peers and SMEs.
Neal
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From: DCHAS-L Discussion List [mailto:dchas-l**At_Symbol_Here**MED.CORNELL.EDU] On Behalf Of Nadejda Spassova
Sent: Thursday, April 02, 2015 1:12 PM
To: DCHAS-L**At_Symbol_Here**MED.CORNELL.EDU
Subject: [DCHAS-L] Nitration, safe work with nitric acid
Hi all,
Recently I start working on a project involving nitration with nitric acid, does anyone has an experience with this kind of reaction ? Also we are mixing nitric acid and acetic acid and then adding the compound to be nitrate, how dangerous is the mixing of the two acids I read that they are incompatible ?
Kind regards,
Nadia
Nadejda Spassova, Ph.D
Research Scientist II, R&D T 514.366.7950ext. 270
F 514.366.5665
9321, Airlie Street, LaSalle, Quebec, Canada H8R 2B2 delmarchem.com
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